Interlayer engineering enhances ion diffusion and structural stability in layered electrode materials for energy storage devices. Layered materials, including oxides and chalcogenides, are crucial for next-gen batteries and supercapacitors. With research on metal-ion (Li +, Na +, K +, Zn 2+, Mg 2+, and Al 3+) batteries based on and beyond rocking-chair mechanism development, more attention has been. . Numerous studies were dedicated to identifying feasible charge storage mechanisms in MXenes and investigating the effects of structural and superficial properties on the corresponding mechanisms. The results clarify that interlayer distance and surface termination groups in MXenes significantly. . To address this issue, we introduce a pristine 2D layer without a polymer matrix to a well-ordered stratificational interlayer by the Langmuir–Blodgett (LB) deposition method, which These systems consist of energy storage units housed in modular containers, typically the size of shipping. . With the constant focus on energy storage devices, layered materials are ideal electrodes for the new generation of highly efficient secondary ion batteries and supercapacitors due to their flexible 2D structures and high theoretical capacities. However, the small interlayer distances in layered. .
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